diff options
-rw-r--r-- | dissertation.cls | 20 | ||||
-rw-r--r-- | dissertation.pdf | bin | 34273364 -> 99920 bytes | |||
-rw-r--r-- | dissertation.syg | 3 | ||||
-rw-r--r-- | dissertation.tex | 34 | ||||
-rw-r--r-- | procedures/chapter.tex | 83 | ||||
-rw-r--r-- | software/chapter.tex | 19 |
6 files changed, 131 insertions, 28 deletions
diff --git a/dissertation.cls b/dissertation.cls index ad59dae..43f1677 100644 --- a/dissertation.cls +++ b/dissertation.cls @@ -31,7 +31,6 @@ \RequirePackage[utf8]{inputenc} \setlength\parindent{0pt} \setlength{\parskip}{1em} -\RequirePackage{enumitem} \setlist{noitemsep, topsep=0pt, parsep=0pt, partopsep=0pt} \renewcommand{\familydefault}{\sfdefault} @@ -39,6 +38,25 @@ \RequirePackage{etoolbox} \AtBeginEnvironment{verse}{\singlespacing} +\RequirePackage[shortlabels]{enumitem} +\newenvironment{denumerate} + { + \begin{enumerate}[topsep=0pt, itemsep=-1ex, partopsep=-10ex, parsep=1ex] + \singlespacing + } + { + \end{enumerate} + } + +\newenvironment{ditemize} + { + \begin{enumerate}[label=$\rightarrow$] + \singlespacing + } + { + \end{enumerate} + } + % --- code environment ---------------------------------------------------------------------------- % \RequirePackage{minted} diff --git a/dissertation.pdf b/dissertation.pdf Binary files differindex 3c85835..e9df137 100644 --- a/dissertation.pdf +++ b/dissertation.pdf diff --git a/dissertation.syg b/dissertation.syg index a878406..e69de29 100644 --- a/dissertation.syg +++ b/dissertation.syg @@ -1,3 +0,0 @@ -\glossaryentry{\ensuremath {N}?\glossentry{N}|setentrycounter[]{page}\glsnumberformat}{8} -\glossaryentry{\ensuremath {N}?\glossentry{N}|setentrycounter[]{page}\glsnumberformat}{8} -\glossaryentry{\ensuremath {\omega }?\glossentry{omega}|setentrycounter[]{page}\glsnumberformat}{36} diff --git a/dissertation.tex b/dissertation.tex index dae87b2..215b039 100644 --- a/dissertation.tex +++ b/dissertation.tex @@ -89,39 +89,39 @@ This dissertation is approved by the following members of the Final Oral Committ % chapters ----------------------------------------------------------------------------------------
-\include{introduction/chapter}
+%\include{introduction/chapter}
\part{Background}
-\include{spectroscopy/chapter}
-\include{materials/chapter}
+%\include{spectroscopy/chapter}
+%\include{materials/chapter}
\include{software/chapter}
\part{Development}
-\include{processing/chapter}
-\include{acquisition/chapter}
-\include{active_correction/chapter}
-\include{opa/chapter}
-\include{mixed_domain/chapter}
+%\include{processing/chapter}
+%\include{acquisition/chapter}
+%\include{active_correction/chapter}
+%\include{opa/chapter}
+%\include{mixed_domain/chapter}
\part{Applications}
-\include{PbSe/chapter}
-\include{MX2/chapter}
+%\include{PbSe/chapter}
+%\include{MX2/chapter}
% TODO: perovskites
-\include{PEDOT:PSS/chapter}
-\include{pyrite/chapter}
-\include{BiVO4/chapter}
+%\include{PEDOT:PSS/chapter}
+%\include{pyrite/chapter}
+%\include{BiVO4/chapter}
% TODO: SPV
% appendix -----------------------------------------------------------------------------------------
\part{Appendix}
\begin{appendix}
-\include{public/chapter}
+%\include{public/chapter}
\include{procedures/chapter}
-\include{hardware/chapter}
+%\include{hardware/chapter}
% TODO: consider inserting WrightTools documentation as PDF
-\include{errata/chapter}
-\include{colophon/chapter}
+%\include{errata/chapter}
+%\include{colophon/chapter}
\end{appendix}
% post --------------------------------------------------------------------------------------------
diff --git a/procedures/chapter.tex b/procedures/chapter.tex index 4ac67ed..9c9bd32 100644 --- a/procedures/chapter.tex +++ b/procedures/chapter.tex @@ -1,5 +1,88 @@ \chapter{Procedures} +\section{Calibrating the 407A} + +Calibrating the 407A + +You may sometimes notice that the zero position changes dramatically from sensitivity to +sensitivity with the 407A. If this happens, iterate through the following until zero stays +consistent: + +Use the fine adjust (knob on side) to zero the 407A on the highest sensitivity + +Use the front adjust (flathead screwdriver needed) to zero on the lowest sensitivity + +\clearpage +\section{Lytron Kodiak RC006} + +We have one Lytron Kodiak RC006: +Model Number RC006G03BB1C002 +Serial Number 739383-02 + +Regular Chiller Maintenance: +\begin{denumerate} + \item Gather supplies. + \begin{enumerate} + \item 1 gallon distilled water (do not use deionized) + \item 1 gallon Nalco 460-PCCL104 (the pink stuff) + \end{enumerate} + \item Drain system completely. + \begin{enumerate} + \item Turn off chiller. + \item Break tubing at push-to-connect, plugging return. + \item Allow chiller to run until liquid stops flowing. You will get a pressure error, ignore + (silence) it. + \item Use tube to mouth-syphon remaining liquid from within chiller + \item Reconnect at push-to-connect + \end{enumerate} + \item Fill chiller with distilled water (should require <1 gallon), let run for 30 minutes. + \item Drain system again. + \item Replace filter. + \item Fill system with one gallon Nalco 460-PCCL104 (the pink stuff). + \item Turn chiller on, top-off with distilled water. + \item Record maintenance, order new supplies for next time if necessary. +\end{denumerate} + +In the past we have had trouble with low flow errors upon system startup. % +These seem to have been fixed by adding a “high” flow loop connecting the outlet and inlet of the +chiller. % +Ideally the pressure drop across this loop is sufficient to still drive fluid through the laser. % + +% TODO: figure + +\clearpage +\section{PolyScience 6000 Series} + +We own two PolyScience chillers---different models but functionally equivalent. + +Grey: Serial Number 3E1161245 + +White and Blue: Serial Number 4K1050550 + +Regular Chiller Maintenance: +\begin{enumerate} + \item Gather supplies +\end{enumerate} + +maintenance directions +Gather supplies +Filter - sold in the stockroom +1 gallon of Nalco 460-PCCL104 (the pink stuff) +Drain system completely +Disconnect red water line and allow chiller to pump water out. +Push nipple of male end with flat object so check valve is released +Take off of filter +Push down to allow water out +Check filters +If air filter dirty, wash with water (let dry after washing) +If water filter is dirty, replace +Reassemble, fill with Nalco 460-PCCL104 (the pink stuff) +Turn chiller on and top-off. + +\section{NesLab Merlin M33} + + + \section{Aligining TOPAS-C} \section{Aligning Spitfire PRO} diff --git a/software/chapter.tex b/software/chapter.tex index 7ad483a..f8ceff7 100644 --- a/software/chapter.tex +++ b/software/chapter.tex @@ -10,13 +10,18 @@ Cutting-edge science increasingly relies on custom software. In their 2008 survey,
\textcite{HannayJoErskine2009a} demonstrated just how important software is to the modern
scientist. %
-\begin{enumerate}[topsep=-1.5ex, itemsep=0ex, partopsep=0ex, parsep=0ex, label=$\rightarrow$]
- \item 84.3\% of surveyed scientists state that developing scientific software is important or very important for their own research.
- \item 91.2\% of surveyed scientists state that using scientific software is important or very important for their own research.
- \item On average, scientists spend approximately 40\% of their work time using scientific software.
- \item On average, scientists spend approximately 30\% of their work time developing scientific software.
-\end{enumerate}
-Despite the importance of software to science and scientists, most scientists are not familiar with basic software engineering concepts.
+\begin{ditemize}
+ \item 84.3\% of surveyed scientists state that developing scientific software is important or
+ very important for their own research.
+ \item 91.2\% of surveyed scientists state that using scientific software is important or very
+ important for their own research.
+ \item On average, scientists spend approximately 40\% of their work time using scientific
+ software.
+ \item On average, scientists spend approximately 30\% of their work time developing scientific
+ software.
+\end{ditemize}
+Despite the importance of software to science and scientists, most scientists are not familiar with
+basic software engineering concepts. %
% TODO: demonstrate that `most scientists are not familiar with basic software engineering concepts'
This is in part due to the their general lack of formal training in programming and software development. \textcite{HannayJoErskine2009a} found that over 90\% of scientists learn software development through `informal self study'. Indeed, I myself have never been formally trained in software development.
|