From 15f4bad7d7441ffee0f118fca2588b93c8d7beb1 Mon Sep 17 00:00:00 2001 From: Philip Lampkin Date: Tue, 18 May 2021 13:03:52 -0500 Subject: Fixed photoreactor base naming, WPP branding and heat inset depth --- photoreactor-base/lightsource_base.f3d | Bin 7380888 -> 0 bytes photoreactor-base/lightsource_base.stl | Bin 1286284 -> 0 bytes photoreactor-base/photoreactor_base.f3d | Bin 0 -> 7510707 bytes photoreactor-base/photoreactor_base.stl | Bin 0 -> 1282584 bytes 4 files changed, 0 insertions(+), 0 deletions(-) delete mode 100644 photoreactor-base/lightsource_base.f3d delete mode 100644 photoreactor-base/lightsource_base.stl create mode 100644 photoreactor-base/photoreactor_base.f3d create mode 100644 photoreactor-base/photoreactor_base.stl diff --git a/photoreactor-base/lightsource_base.f3d b/photoreactor-base/lightsource_base.f3d deleted file mode 100644 index 05ba109..0000000 Binary files a/photoreactor-base/lightsource_base.f3d and /dev/null differ diff --git a/photoreactor-base/lightsource_base.stl b/photoreactor-base/lightsource_base.stl deleted file mode 100644 index 5025f37..0000000 Binary files a/photoreactor-base/lightsource_base.stl and /dev/null differ diff --git a/photoreactor-base/photoreactor_base.f3d b/photoreactor-base/photoreactor_base.f3d new file mode 100644 index 0000000..b209d98 Binary files /dev/null and b/photoreactor-base/photoreactor_base.f3d differ diff --git a/photoreactor-base/photoreactor_base.stl b/photoreactor-base/photoreactor_base.stl new file mode 100644 index 0000000..0536fb2 Binary files /dev/null and b/photoreactor-base/photoreactor_base.stl differ -- cgit v1.2.3 From c2b6448e1a3a82b3eb86cde21caaa1c94c6ee988 Mon Sep 17 00:00:00 2001 From: plampkin <83132062+plampkin@users.noreply.github.com> Date: Tue, 18 May 2021 13:38:24 -0500 Subject: Updated README.md Added correct manufacturer part numbers --- photoreactor-reaction-modules/README.md | 10 +++++----- 1 file changed, 5 insertions(+), 5 deletions(-) diff --git a/photoreactor-reaction-modules/README.md b/photoreactor-reaction-modules/README.md index 694a7a3..1b87fc0 100644 --- a/photoreactor-reaction-modules/README.md +++ b/photoreactor-reaction-modules/README.md @@ -13,11 +13,11 @@ CAD designs and 3D-printable models for modules compatible with various common r | vessel | manufacturer | manufacturer part number | | :------------- | :----------------- | :------------------------ | -| 1 mL Vial | Fisher Scientific | IN-C39CTOU2 | -| 4 mL Vial | Chemglass | IN-C39CTOU5 | -| 8 mL Vial | Chemglass | XTEARY-00-0000-000000N09 | -| 10 mL Schlenk | Synthware | LXML-PE01-0080 | -| 24 mL Vial | VWR | XPEBGR-L1-0000-00D01 | +| 2 mL Vial | Fisher Scientific | 03-338AA | +| 4 mL Vial | Chemglass | CG-4909-04 | +| 8 mL Vial | Chemglass | CG-4909-03 | +| 10 mL Schlenk | Synthware | F580010 | +| 24 mL Vial | VWR | Vial: VWR 66012-044 Cap: Chemglass CG-4911-20 | ## Bill of Materials -- cgit v1.2.3 From 42d1d150efc65c5a4ae86aac651b5025b1c31bb6 Mon Sep 17 00:00:00 2001 From: Philip Lampkin Date: Tue, 18 May 2021 13:43:46 -0500 Subject: updated 1mL to 2mL and item number --- .../1mL-03-338A-chamber.f3d | Bin 233120 -> 0 bytes .../1mL-03-338A-chamber.stl | Bin 27284 -> 0 bytes .../1mL-03-338A-holder.f3d | Bin 4180970 -> 0 bytes .../1mL-03-338A-holder.stl | Bin 748284 -> 0 bytes .../2mL-03-338AA-chamber.f3d | Bin 0 -> 233120 bytes .../2mL-03-338AA-chamber.stl | Bin 0 -> 27284 bytes .../2mL-03-338AA-holder.f3d | Bin 0 -> 4180970 bytes .../2mL-03-338AA-holder.stl | Bin 0 -> 748284 bytes 8 files changed, 0 insertions(+), 0 deletions(-) delete mode 100644 photoreactor-reaction-modules/1ml-vial-Fisher-Scientific-03-338A/1mL-03-338A-chamber.f3d delete mode 100644 photoreactor-reaction-modules/1ml-vial-Fisher-Scientific-03-338A/1mL-03-338A-chamber.stl delete mode 100644 photoreactor-reaction-modules/1ml-vial-Fisher-Scientific-03-338A/1mL-03-338A-holder.f3d delete mode 100644 photoreactor-reaction-modules/1ml-vial-Fisher-Scientific-03-338A/1mL-03-338A-holder.stl create mode 100644 photoreactor-reaction-modules/2ml-vial-Fisher-Scientific-03-338AA/2mL-03-338AA-chamber.f3d create mode 100644 photoreactor-reaction-modules/2ml-vial-Fisher-Scientific-03-338AA/2mL-03-338AA-chamber.stl create mode 100644 photoreactor-reaction-modules/2ml-vial-Fisher-Scientific-03-338AA/2mL-03-338AA-holder.f3d create mode 100644 photoreactor-reaction-modules/2ml-vial-Fisher-Scientific-03-338AA/2mL-03-338AA-holder.stl diff --git a/photoreactor-reaction-modules/1ml-vial-Fisher-Scientific-03-338A/1mL-03-338A-chamber.f3d b/photoreactor-reaction-modules/1ml-vial-Fisher-Scientific-03-338A/1mL-03-338A-chamber.f3d deleted file mode 100644 index 7f2cc3d..0000000 Binary files a/photoreactor-reaction-modules/1ml-vial-Fisher-Scientific-03-338A/1mL-03-338A-chamber.f3d and /dev/null differ diff --git a/photoreactor-reaction-modules/1ml-vial-Fisher-Scientific-03-338A/1mL-03-338A-chamber.stl 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a/photoreactor-reaction-modules/2ml-vial-Fisher-Scientific-03-338AA/2mL-03-338AA-chamber.f3d b/photoreactor-reaction-modules/2ml-vial-Fisher-Scientific-03-338AA/2mL-03-338AA-chamber.f3d new file mode 100644 index 0000000..7f2cc3d Binary files /dev/null and b/photoreactor-reaction-modules/2ml-vial-Fisher-Scientific-03-338AA/2mL-03-338AA-chamber.f3d differ diff --git a/photoreactor-reaction-modules/2ml-vial-Fisher-Scientific-03-338AA/2mL-03-338AA-chamber.stl b/photoreactor-reaction-modules/2ml-vial-Fisher-Scientific-03-338AA/2mL-03-338AA-chamber.stl new file mode 100644 index 0000000..08da6cd Binary files /dev/null and b/photoreactor-reaction-modules/2ml-vial-Fisher-Scientific-03-338AA/2mL-03-338AA-chamber.stl differ diff --git a/photoreactor-reaction-modules/2ml-vial-Fisher-Scientific-03-338AA/2mL-03-338AA-holder.f3d b/photoreactor-reaction-modules/2ml-vial-Fisher-Scientific-03-338AA/2mL-03-338AA-holder.f3d new file mode 100644 index 0000000..8648f69 Binary files /dev/null and b/photoreactor-reaction-modules/2ml-vial-Fisher-Scientific-03-338AA/2mL-03-338AA-holder.f3d differ diff --git a/photoreactor-reaction-modules/2ml-vial-Fisher-Scientific-03-338AA/2mL-03-338AA-holder.stl b/photoreactor-reaction-modules/2ml-vial-Fisher-Scientific-03-338AA/2mL-03-338AA-holder.stl new file mode 100644 index 0000000..286783f Binary files /dev/null and b/photoreactor-reaction-modules/2ml-vial-Fisher-Scientific-03-338AA/2mL-03-338AA-holder.stl differ -- cgit v1.2.3 From bee7ce30cba814ae099963cb2859f4e7bd672db7 Mon Sep 17 00:00:00 2001 From: plampkin <83132062+plampkin@users.noreply.github.com> Date: Tue, 18 May 2021 13:56:43 -0500 Subject: Update README.md Added extra vendors for LDD-1000L driver --- analog-driver-board/README.md | 2 +- 1 file changed, 1 insertion(+), 1 deletion(-) diff --git a/analog-driver-board/README.md b/analog-driver-board/README.md index 43ee059..5ba9b29 100644 --- a/analog-driver-board/README.md +++ b/analog-driver-board/README.md @@ -31,7 +31,7 @@ PCB images generated with [tracespace](https://github.com/tracespace/tracespace) | TP1 | (yellow) | Keystone | 5014 | $0.50 | [DigiKey](https://www.digikey.com/en/products/detail/keystone-electronics/5014/255336) | | TP2 | (red) | Keystone | 5010 | $0.50 | [DigiKey](https://www.digikey.com/en/products/detail/keystone-electronics/5010/255332) | | TP3 | (black) | Keystone | 5011 | $0.50 | [DigiKey](https://www.digikey.com/en/products/detail/keystone-electronics/5011/255333) | | -| U2 | LED driver | Mean Well | LDD-1000L | $6.00 | [DigiKey](https://www.digikey.com/en/products/detail/mean-well-usa-inc/LDD-1000L/7704722) [Allied](https://www.alliedelec.com/product/mean-well/ldd-1000l/70345765/) | +| U2 | LED driver | Mean Well | LDD-1000L | $6.00 | [DigiKey](https://www.digikey.com/en/products/detail/mean-well-usa-inc/LDD-1000L/7704722) [Allied](https://www.alliedelec.com/product/mean-well/ldd-1000l/70345765/) [Mouser](https://www.mouser.com/ProductDetail/MEAN-WELL/LDD-1000L?qs=JK6Bpmia%2FmvDNI%252Ba1vDDrA%3D%3D) [Newark](https://www.newark.com/mean-well/ldd-1000l/dc-dc-converter-analog-pwm-30w/dp/14AJ2201) [LEDSupply](https://www.ledsupply.com/led-drivers/mean-well-ldd-l-series-cc-step-down-mode)| All prices are extended estimates in USD. In general, these are overestimates, so this should be an upper-estimate on cost. -- cgit v1.2.3 From 7c35fa651acb73fa0c590ba09e2f9f0582f8c7e3 Mon Sep 17 00:00:00 2001 From: plampkin <83132062+plampkin@users.noreply.github.com> Date: Tue, 18 May 2021 14:05:53 -0500 Subject: Update README.md added LDD-1000L vendors --- digital-driver-board/README.md | 2 +- 1 file changed, 1 insertion(+), 1 deletion(-) diff --git a/digital-driver-board/README.md b/digital-driver-board/README.md index 0b60d67..766699f 100644 --- a/digital-driver-board/README.md +++ b/digital-driver-board/README.md @@ -29,7 +29,7 @@ Bill of Materials | R2, R5 | 470 | Yageo | RC1206FR-07470RL | $0.10 | [DigiKey](https://www.digikey.com/en/products/detail/yageo/RC1206FR-07470RL/728934) | | R3 | 10k | Yageo | RC1206FR-0710KL | $0.10 | [DigiKey](https://www.digikey.com/en/products/detail/yageo/RC1206FR-0710KL/728483) | | U1 | microcontrol. | Microchip | ATTINY85-20PU | $1.50 | [DigiKey](https://www.digikey.com/en/products/detail/microchip-technology/attiny85-20pu/735469) [Newark](https://www.newark.com/microchip/attiny85-20pu/microcontroller-mcu-8-bit-attiny/dp/68T3808) | -| U2 | LED driver | Mean Well | LDD-1000L | $6.00 | [DigiKey](https://www.digikey.com/en/products/detail/mean-well-usa-inc/LDD-1000L/7704722) [Allied](https://www.alliedelec.com/product/mean-well/ldd-1000l/70345765/) | +| U2 | LED driver | Mean Well | LDD-1000L | $6.00 | [DigiKey](https://www.digikey.com/en/products/detail/mean-well-usa-inc/LDD-1000L/7704722) [Allied](https://www.alliedelec.com/product/mean-well/ldd-1000l/70345765/) [Mouser](https://www.mouser.com/ProductDetail/MEAN-WELL/LDD-1000L?qs=JK6Bpmia%2FmvDNI%252Ba1vDDrA%3D%3D) [Newark](https://www.newark.com/mean-well/ldd-1000l/dc-dc-converter-analog-pwm-30w/dp/14AJ2201) [LEDSupply](https://www.ledsupply.com/led-drivers/mean-well-ldd-l-series-cc-step-down-mode)| ## I2C Interface -- cgit v1.2.3 From 47d4a62b052ae3ac83892462ffca3c2622413dbd Mon Sep 17 00:00:00 2001 From: Philip Lampkin Date: Tue, 18 May 2021 14:14:05 -0500 Subject: updated fab guide 1mL to 2mL --- .../wpp-fabrication-operation.pdf | Bin 44331888 -> 44331987 bytes .../wpp-fabrication-operation.tex | 6 +++--- 2 files changed, 3 insertions(+), 3 deletions(-) diff --git a/fabrication-and-operation-instructions/wpp-fabrication-operation.pdf b/fabrication-and-operation-instructions/wpp-fabrication-operation.pdf index 571ccd2..36269dc 100644 Binary files a/fabrication-and-operation-instructions/wpp-fabrication-operation.pdf and b/fabrication-and-operation-instructions/wpp-fabrication-operation.pdf differ diff --git a/fabrication-and-operation-instructions/wpp-fabrication-operation.tex b/fabrication-and-operation-instructions/wpp-fabrication-operation.tex index e9cef7d..a6eef05 100644 --- a/fabrication-and-operation-instructions/wpp-fabrication-operation.tex +++ b/fabrication-and-operation-instructions/wpp-fabrication-operation.tex @@ -216,12 +216,12 @@ Remember to use proper eye protection. \begin{figure}[H] \includegraphics[width=\textwidth]{"./fig8.png"} - \caption{(A) Provided reaction modules for 1-, 4-, 8- and 24-mL vials. (B) WPP devices fitted with the provided reaction modules. (C) Single and (D) multiple reaction configurations for provide 4-mL module.} + \caption{(A) Provided reaction modules for 2-, 4-, 8- and 24-mL vials. (B) WPP devices fitted with the provided reaction modules. (C) Single and (D) multiple reaction configurations for provide 4-mL module.} \end{figure} A WPP reaction module consists of a reaction chamber and vessel holder. By modifying chamber height and adjusting holder geometry, one can produce modules compatible with reaction vessels of various types and sizes. -Fusion360 designs and stl models for modules compatible with 1-, 4-, 8- and 24-mL vials are provided in the 'photoreaction-modules' subdirectory of the project repository (Figure 8A—B). +Fusion360 designs and stl models for modules compatible with 2-, 4-, 8- and 24-mL vials are provided in the 'photoreaction-modules' subdirectory of the project repository (Figure 8A—B). Template reaction chamber and vessel holder Fusion360 designs are provided in the same directory. We encourage you to design your own reaction modules if those provided in the project repository do not meet your needs. @@ -594,7 +594,7 @@ WPP reactors utilize high-intensity light emitting diodes (LED) that can cause e Light-filtering safety glasses should be worn whenever a WPP apparatus photon source is powered. Care must be taken to use safety glasses protective against the specific emission wavelengths of the photon source. -\section{Acknowledgements} +\section{Acknowledgments} We thank Dr. Ilia Guzei for photography. We are grateful to Sebastian Thompson for help in production of custom LED stars. -- cgit v1.2.3 From 246b82b5dfb0003dcab7031b7fe9decbc580ac70 Mon Sep 17 00:00:00 2001 From: plampkin <83132062+plampkin@users.noreply.github.com> Date: Tue, 18 May 2021 14:31:24 -0500 Subject: Update README.md added links to LED stars from LEDsupply --- photon-source-leds/README.md | 22 +++++++++++----------- 1 file changed, 11 insertions(+), 11 deletions(-) diff --git a/photon-source-leds/README.md b/photon-source-leds/README.md index 9627bad..9b3740b 100644 --- a/photon-source-leds/README.md +++ b/photon-source-leds/README.md @@ -8,17 +8,17 @@ WPP-compatible custom LED stars mounted with 3.5 mm surface mount LEDs of any wa ## List of compatible commercial LED stars -| color | max emission | manufacturer | manufacturer part number | LEDsupply LED star part number | LEDsupply price | Other vendors | -| :------------- | :----------- | :----------- | :----------------------- | :----------------------------- | :-------------- |:------------- | -| UVA | 365 nm | Inolux | IN-C39CTOU2 | N/A (mounted by user) | N/A | [DigiKey](https://www.digikey.com/en/products/detail/inolux/IN-C39CTOU2/9681227) [Mouser](https://www.mouser.com/ProductDetail/Inolux/IN-C39CTOU2/?qs=qSfuJ%252Bfl%2Fd4759YPTEyoag%3D%3D) | -| Violet | 400 nm | Inolux | IN-C39CTOU5 | N/A (mounted by user) | N/A | [DigiKey](https://www.digikey.com/en/products/detail/inolux/IN-C39CTOU5/9681233) [Mouser](https://www.mouser.com/ProductDetail/Inolux/IN-C39CTOU5/?qs=qSfuJ%252Bfl%2Fd6BLbca08ZG2g%3D%3D) | -| Blue | 450 nm | Cree, Inc. | XTEARY-00-0000-000000N09 | CREEXTE-ROY-3 | $10.10 | [DigiKey](https://www.digikey.com/en/products/detail/cree-inc/XTEARY-00-0000-000000N09/3744336) [Mouser](https://www.mouser.com/ProductDetail/Cree-Inc/XTEARY-00-0000-000000N09?qs=ygRr%2Ftkhtevu4HqMzfGc3w%3D%3D) | -| Cyan | 495 nm | Luxeon | LXML-PE01-0080 | 07007-PE000-K | $12.60 | [DigiKey](https://www.digikey.com/en/products/detail/lumileds/LXML-PE01-0080/3961255) [Mouser](https://www.mouser.com/ProductDetail/Lumileds/LXML-PE01-0080/?qs=7Vwje68bFtO%2F0g2M%252BAMdYQ%3D%3D) | -| Green | 530 nm | Cree, Inc. | XPEBGR-L1-0000-00D01 | CREEXPE2-GRN-3 | $10.50 | [DigiKey](https://www.digikey.com/en/products/detail/cree-inc/XPEBGR-L1-0000-00D01/4177200) [Mouser](https://www.mouser.com/ProductDetail/Cree-Inc/XPEBGR-L1-0000-00D01/?qs=rHlcMk0NooK%2FtCgm9PQ0pQ%3D%3D) | -| Amber | 590 nm | Luxeon | LXML-PL01-0060 | 07007-PL000-F | $12.60 | [DigiKey](https://www.digikey.com/en/products/detail/lumileds/LXML-PL01-0050/3961256) [Mouser](https://www.mouser.com/ProductDetail/Lumileds/LXML-PL01-0060?qs=7Vwje68bFtP0H6dN9OA%2FuA%3D%3D) | -| Orange | 620 nm | Cree, Inc. | XPEBRO-L1-0000-00901 | CREEXPE2-RDO-3 | $10.50 | [DigiKey](https://www.digikey.com/en/products/detail/cree-inc/XPEBRO-L1-0000-00901/4177164) [Mouser](https://www.mouser.com/ProductDetail/Cree-Inc/XPEBRO-L1-0000-00901?qs=rHlcMk0NooLQklUEc3IqMg%3D%3D) | -| Red | 660 nm | Cree, Inc. | XPEPHR-L1-0000-00801 | CREEXPE-DRD-3 | $10.50 | [DigiKey](https://www.digikey.com/en/products/detail/cree-inc/XPEPHR-L1-0000-00801/4895013) [Mouser](https://www.mouser.com/ProductDetail/Cree-Inc/XPEPHR-L1-0000-00801/?qs=3izLlwrMQ7lAtbsWL38zog%3D%3D) | -| NIR | 730 nm | Cree, Inc. | XPEFAR-L1-0000-00601 | CREEXPE-FRD-3 | $12.00 | [DigiKey](https://www.digikey.com/en/products/detail/cree-inc/XPEFAR-L1-0000-00601/5303643) [Mouser](https://www.mouser.com/ProductDetail/Cree-Inc/XPEFAR-L1-0000-00601?qs=k72kBymvut%252B0JKg4b6%252BzNg%3D%3D) | +| color | max emission | manufacturer | manufacturer part number | LEDsupply LED star part number | LEDsupply price | LED Star vendors | LED vendors | +| :------------- | :----------- | :----------- | :----------------------- | :----------------------------- | :-------------- | :--------------- | :------------ | +| UVA | 365 nm | Inolux | IN-C39CTOU2 | N/A (mounted by user) | N/A | N/A | [DigiKey](https://www.digikey.com/en/products/detail/inolux/IN-C39CTOU2/9681227) [Mouser](https://www.mouser.com/ProductDetail/Inolux/IN-C39CTOU2/?qs=qSfuJ%252Bfl%2Fd4759YPTEyoag%3D%3D) | +| Violet | 400 nm | Inolux | IN-C39CTOU5 | N/A (mounted by user) | N/A | N/A | [DigiKey](https://www.digikey.com/en/products/detail/inolux/IN-C39CTOU5/9681233) [Mouser](https://www.mouser.com/ProductDetail/Inolux/IN-C39CTOU5/?qs=qSfuJ%252Bfl%2Fd6BLbca08ZG2g%3D%3D) | +| Blue | 450 nm | Cree, Inc. | XTEARY-00-0000-000000N09 | CREEXTE-ROY-3 | $10.10 | [LEDSupply](https://www.ledsupply.com/leds/cree-xlamp-xt-e-royal-blue-leds) | [DigiKey](https://www.digikey.com/en/products/detail/cree-inc/XTEARY-00-0000-000000N09/3744336) [Mouser](https://www.mouser.com/ProductDetail/Cree-Inc/XTEARY-00-0000-000000N09?qs=ygRr%2Ftkhtevu4HqMzfGc3w%3D%3D) | +| Cyan | 495 nm | Luxeon | LXML-PE01-0080 | 07007-PE000-K | $12.60 | [LEDSupply](https://www.ledsupply.com/leds/luxeon-rebel-color-leds) | [DigiKey](https://www.digikey.com/en/products/detail/lumileds/LXML-PE01-0080/3961255) [Mouser](https://www.mouser.com/ProductDetail/Lumileds/LXML-PE01-0080/?qs=7Vwje68bFtO%2F0g2M%252BAMdYQ%3D%3D) | +| Green | 530 nm | Cree, Inc. | XPEBGR-L1-0000-00D01 | CREEXPE2-GRN-3 | $10.50 | [LEDSupply](https://www.ledsupply.com/leds/cree-xlamp-xp-e2-color-high-power-led-star) | [DigiKey](https://www.digikey.com/en/products/detail/cree-inc/XPEBGR-L1-0000-00D01/4177200) [Mouser](https://www.mouser.com/ProductDetail/Cree-Inc/XPEBGR-L1-0000-00D01/?qs=rHlcMk0NooK%2FtCgm9PQ0pQ%3D%3D) | +| Amber | 590 nm | Luxeon | LXML-PL01-0060 | 07007-PL000-F | $12.60 | [LEDSupply](https://www.ledsupply.com/leds/luxeon-rebel-color-leds) | [DigiKey](https://www.digikey.com/en/products/detail/lumileds/LXML-PL01-0050/3961256) [Mouser](https://www.mouser.com/ProductDetail/Lumileds/LXML-PL01-0060?qs=7Vwje68bFtP0H6dN9OA%2FuA%3D%3D) | +| Orange | 620 nm | Cree, Inc. | XPEBRO-L1-0000-00901 | CREEXPE2-RDO-3 | $10.50 | [LEDSupply](https://www.ledsupply.com/leds/cree-xlamp-xp-e2-color-high-power-led-star) | [DigiKey](https://www.digikey.com/en/products/detail/cree-inc/XPEBRO-L1-0000-00901/4177164) [Mouser](https://www.mouser.com/ProductDetail/Cree-Inc/XPEBRO-L1-0000-00901?qs=rHlcMk0NooLQklUEc3IqMg%3D%3D) | +| Red | 660 nm | Cree, Inc. | XPEPHR-L1-0000-00801 | CREEXPE-DRD-3 | $10.50 | [LEDSupply](https://www.ledsupply.com/leds/cree-xlamp-xpe-high-power-led-star) | [DigiKey](https://www.digikey.com/en/products/detail/cree-inc/XPEPHR-L1-0000-00801/4895013) [Mouser](https://www.mouser.com/ProductDetail/Cree-Inc/XPEPHR-L1-0000-00801/?qs=3izLlwrMQ7lAtbsWL38zog%3D%3D) | +| NIR | 730 nm | Cree, Inc. | XPEFAR-L1-0000-00601 | CREEXPE-FRD-3 | $12.00 | [LEDSupply](https://www.ledsupply.com/leds/cree-xlamp-xpe-high-power-led-star) | [DigiKey](https://www.digikey.com/en/products/detail/cree-inc/XPEFAR-L1-0000-00601/5303643) [Mouser](https://www.mouser.com/ProductDetail/Cree-Inc/XPEFAR-L1-0000-00601?qs=k72kBymvut%252B0JKg4b6%252BzNg%3D%3D) | All prices are in USD. In general, prices are overestimates, thereby providing an upper estimate on cost. -- cgit v1.2.3 From 4a87549f9af6d97a379e1cfc27fe08cfcf055bd0 Mon Sep 17 00:00:00 2001 From: plampkin <83132062+plampkin@users.noreply.github.com> Date: Tue, 18 May 2021 21:43:50 -0500 Subject: Update README.md --- README.md | 4 ++-- 1 file changed, 2 insertions(+), 2 deletions(-) diff --git a/README.md b/README.md index 1751eeb..ce79834 100644 --- a/README.md +++ b/README.md @@ -19,10 +19,10 @@ This repository is being mirrored to several version control systems in an attem ## Safety -The Wisconsin Photoreactor is for use by trained chemists. +The Wisconsin Photoreactor Platform is for use by trained chemists. WPP apparatuses utilize high-intensity light emitting diodes (LED) that can cause eye damage if proper safety precautions are not observed. -Light-filtering safety glasses should be worn whenever a WPP apparatus photon source is powered. +Light-filtering safety glasses should be worn whenever a WPP apparatus photon source is powered. Care must be taken to use safety glasses protective against the specific emission wavelengths of a photon source. ## Fabrication and Operation Instructions -- cgit v1.2.3 From c74fd589667d0aa1c3c0496e302e3938ee3bb3bf Mon Sep 17 00:00:00 2001 From: plampkin <83132062+plampkin@users.noreply.github.com> Date: Tue, 18 May 2021 21:47:05 -0500 Subject: Update README.md --- analog-driver-board/README.md | 6 +++--- 1 file changed, 3 insertions(+), 3 deletions(-) diff --git a/analog-driver-board/README.md b/analog-driver-board/README.md index 5ba9b29..82dae13 100644 --- a/analog-driver-board/README.md +++ b/analog-driver-board/README.md @@ -1,6 +1,6 @@ # Analog Driver Board -A simple photoreactor driver board providing control of light intensity. This control is achieved through adjustment of the board-mounted potentiometer. No software is required, and multiple WPP reactors fitted with this board can be connected in series to a single power source. However, fan speed isn’t adjustable and is maintained at maximum. +A simple photoreactor driver board providing control over light intensity. This control is achieved through adjustment of the board-mounted potentiometer. No software is required, and multiple WPP reactors fitted with this board can be connected in series to a single power source. However, fan speed isn’t adjustable and is maintained at maximum. Relative light intensity can be determined using the analog driver board test points and a multimeter. See operation instructions for more information. @@ -31,7 +31,7 @@ PCB images generated with [tracespace](https://github.com/tracespace/tracespace) | TP1 | (yellow) | Keystone | 5014 | $0.50 | [DigiKey](https://www.digikey.com/en/products/detail/keystone-electronics/5014/255336) | | TP2 | (red) | Keystone | 5010 | $0.50 | [DigiKey](https://www.digikey.com/en/products/detail/keystone-electronics/5010/255332) | | TP3 | (black) | Keystone | 5011 | $0.50 | [DigiKey](https://www.digikey.com/en/products/detail/keystone-electronics/5011/255333) | | -| U2 | LED driver | Mean Well | LDD-1000L | $6.00 | [DigiKey](https://www.digikey.com/en/products/detail/mean-well-usa-inc/LDD-1000L/7704722) [Allied](https://www.alliedelec.com/product/mean-well/ldd-1000l/70345765/) [Mouser](https://www.mouser.com/ProductDetail/MEAN-WELL/LDD-1000L?qs=JK6Bpmia%2FmvDNI%252Ba1vDDrA%3D%3D) [Newark](https://www.newark.com/mean-well/ldd-1000l/dc-dc-converter-analog-pwm-30w/dp/14AJ2201) [LEDSupply](https://www.ledsupply.com/led-drivers/mean-well-ldd-l-series-cc-step-down-mode)| +| U2 | LED driver | Mean Well | LDD-1000L (pin) | $6.00 | [DigiKey](https://www.digikey.com/en/products/detail/mean-well-usa-inc/LDD-1000L/7704722) [Allied](https://www.alliedelec.com/product/mean-well/ldd-1000l/70345765/) [Mouser](https://www.mouser.com/ProductDetail/MEAN-WELL/LDD-1000L?qs=JK6Bpmia%2FmvDNI%252Ba1vDDrA%3D%3D) [Newark](https://www.newark.com/mean-well/ldd-1000l/dc-dc-converter-analog-pwm-30w/dp/14AJ2201) [LEDSupply](https://www.ledsupply.com/led-drivers/mean-well-ldd-l-series-cc-step-down-mode)| All prices are extended estimates in USD. In general, these are overestimates, so this should be an upper-estimate on cost. @@ -43,7 +43,7 @@ Boards themselves can be printed for approximately $5 each. ### Unprinted ### Changed -- removed wisconsin crest logo +- Removed wisconsin crest logo ### Revision B -- cgit v1.2.3 From 10c22b1a0a646d6d53678f9d9e5a3b1464953cbe Mon Sep 17 00:00:00 2001 From: Philip Lampkin Date: Tue, 18 May 2021 21:53:03 -0500 Subject: fixed naming conventions --- .../wpp-fabrication-operation.pdf | Bin 44331987 -> 44332175 bytes .../wpp-fabrication-operation.tex | 8 +++----- photon-source-leds/Cyan-495 nm-LXML-PE01-0080.png | Bin 183864 -> 0 bytes photon-source-leds/Cyan-495-nm-LXML-PE01-0080.png | Bin 0 -> 183864 bytes 4 files changed, 3 insertions(+), 5 deletions(-) delete mode 100644 photon-source-leds/Cyan-495 nm-LXML-PE01-0080.png create mode 100644 photon-source-leds/Cyan-495-nm-LXML-PE01-0080.png diff --git a/fabrication-and-operation-instructions/wpp-fabrication-operation.pdf b/fabrication-and-operation-instructions/wpp-fabrication-operation.pdf index 36269dc..12069aa 100644 Binary files a/fabrication-and-operation-instructions/wpp-fabrication-operation.pdf and b/fabrication-and-operation-instructions/wpp-fabrication-operation.pdf differ diff --git a/fabrication-and-operation-instructions/wpp-fabrication-operation.tex b/fabrication-and-operation-instructions/wpp-fabrication-operation.tex index a6eef05..0ceeb4e 100644 --- a/fabrication-and-operation-instructions/wpp-fabrication-operation.tex +++ b/fabrication-and-operation-instructions/wpp-fabrication-operation.tex @@ -53,11 +53,9 @@ % title \title{Wisconsin Photoreactor Platform\\Fabrication and Operation Guide} -\author{ - Philip P. Lampkin \\ - Blaise J. Thompson \\ - Samuel H. Gellman - } + +\author{Philip P. Lampkin, Blaise J. Thompson, Samuel H. Gellman*} + \date{\today} \begin{document} diff --git a/photon-source-leds/Cyan-495 nm-LXML-PE01-0080.png b/photon-source-leds/Cyan-495 nm-LXML-PE01-0080.png deleted file mode 100644 index 95ed24a..0000000 Binary files a/photon-source-leds/Cyan-495 nm-LXML-PE01-0080.png and /dev/null differ diff --git a/photon-source-leds/Cyan-495-nm-LXML-PE01-0080.png b/photon-source-leds/Cyan-495-nm-LXML-PE01-0080.png new file mode 100644 index 0000000..95ed24a Binary files /dev/null and b/photon-source-leds/Cyan-495-nm-LXML-PE01-0080.png differ -- cgit v1.2.3 From eeeadbc6122dddf3ec5c2c7329a907d943feb2ba Mon Sep 17 00:00:00 2001 From: plampkin <83132062+plampkin@users.noreply.github.com> Date: Tue, 18 May 2021 21:54:31 -0500 Subject: Update README.md --- photon-source-leds/README.md | 4 ++-- 1 file changed, 2 insertions(+), 2 deletions(-) diff --git a/photon-source-leds/README.md b/photon-source-leds/README.md index f19645e..22386fd 100644 --- a/photon-source-leds/README.md +++ b/photon-source-leds/README.md @@ -11,11 +11,11 @@ WPP-compatible custom LED stars mounted with 3.5 mm surface mount LEDs of any wa | color | max emission | manufacturer | manufacturer part number | LEDsupply LED star part number | LEDsupply price | LED Star vendors | LED vendors | | :------------- | :----------- | :----------- | :----------------------- | :----------------------------- | :-------------- | :--------------- | :------------ | | UVA | 365 nm | Inolux | IN-C39CTOU2 | N/A (mounted by user) | N/A | N/A | [DigiKey](https://www.digikey.com/en/products/detail/inolux/IN-C39CTOU2/9681227) [Mouser](https://www.mouser.com/ProductDetail/Inolux/IN-C39CTOU2/?qs=qSfuJ%252Bfl%2Fd4759YPTEyoag%3D%3D) | -| Violet | 400 nm | Inolux | IN-C39CTOU5 | N/A (mounted by user) | N/A | N/A | [DigiKey](https://www.digikey.com/en/products/detail/inolux/IN-C39CTOU5/9681233) [Mouser](https://www.mouser.com/ProductDetail/Inolux/IN-C39CTOU5/?qs=qSfuJ%252Bfl%2Fd6BLbca08ZG2g%3D%3D) | +| Violet | 395 nm | Inolux | IN-C39CTOU5 | N/A (mounted by user) | N/A | N/A | [DigiKey](https://www.digikey.com/en/products/detail/inolux/IN-C39CTOU5/9681233) [Mouser](https://www.mouser.com/ProductDetail/Inolux/IN-C39CTOU5/?qs=qSfuJ%252Bfl%2Fd6BLbca08ZG2g%3D%3D) | | Blue | 450 nm | Cree, Inc. | XTEARY-00-0000-000000N09 | CREEXTE-ROY-3 | $10.10 | [LEDSupply](https://www.ledsupply.com/leds/cree-xlamp-xt-e-royal-blue-leds) | [DigiKey](https://www.digikey.com/en/products/detail/cree-inc/XTEARY-00-0000-000000N09/3744336) [Mouser](https://www.mouser.com/ProductDetail/Cree-Inc/XTEARY-00-0000-000000N09?qs=ygRr%2Ftkhtevu4HqMzfGc3w%3D%3D) | | Cyan | 495 nm | Luxeon | LXML-PE01-0080 | 07007-PE000-K | $12.60 | [LEDSupply](https://www.ledsupply.com/leds/luxeon-rebel-color-leds) | [DigiKey](https://www.digikey.com/en/products/detail/lumileds/LXML-PE01-0080/3961255) [Mouser](https://www.mouser.com/ProductDetail/Lumileds/LXML-PE01-0080/?qs=7Vwje68bFtO%2F0g2M%252BAMdYQ%3D%3D) | | Green | 530 nm | Cree, Inc. | XPEBGR-L1-0000-00D01 | CREEXPE2-GRN-3 | $10.50 | [LEDSupply](https://www.ledsupply.com/leds/cree-xlamp-xp-e2-color-high-power-led-star) | [DigiKey](https://www.digikey.com/en/products/detail/cree-inc/XPEBGR-L1-0000-00D01/4177200) [Mouser](https://www.mouser.com/ProductDetail/Cree-Inc/XPEBGR-L1-0000-00D01/?qs=rHlcMk0NooK%2FtCgm9PQ0pQ%3D%3D) | -| Amber | 590 nm | Luxeon | LXML-PL01-0060 | 07007-PL000-F | $12.60 | [LEDSupply](https://www.ledsupply.com/leds/luxeon-rebel-color-leds) | [DigiKey](https://www.digikey.com/en/products/detail/lumileds/LXML-PL01-0050/3961256) [Mouser](https://www.mouser.com/ProductDetail/Lumileds/LXML-PL01-0060?qs=7Vwje68bFtP0H6dN9OA%2FuA%3D%3D) | +| Amber | 595 nm | Luxeon | LXML-PL01-0060 | 07007-PL000-F | $12.60 | [LEDSupply](https://www.ledsupply.com/leds/luxeon-rebel-color-leds) | [DigiKey](https://www.digikey.com/en/products/detail/lumileds/LXML-PL01-0050/3961256) [Mouser](https://www.mouser.com/ProductDetail/Lumileds/LXML-PL01-0060?qs=7Vwje68bFtP0H6dN9OA%2FuA%3D%3D) | | Orange | 620 nm | Cree, Inc. | XPEBRO-L1-0000-00901 | CREEXPE2-RDO-3 | $10.50 | [LEDSupply](https://www.ledsupply.com/leds/cree-xlamp-xp-e2-color-high-power-led-star) | [DigiKey](https://www.digikey.com/en/products/detail/cree-inc/XPEBRO-L1-0000-00901/4177164) [Mouser](https://www.mouser.com/ProductDetail/Cree-Inc/XPEBRO-L1-0000-00901?qs=rHlcMk0NooLQklUEc3IqMg%3D%3D) | | Red | 660 nm | Cree, Inc. | XPEPHR-L1-0000-00801 | CREEXPE-DRD-3 | $10.50 | [LEDSupply](https://www.ledsupply.com/leds/cree-xlamp-xpe-high-power-led-star) | [DigiKey](https://www.digikey.com/en/products/detail/cree-inc/XPEPHR-L1-0000-00801/4895013) [Mouser](https://www.mouser.com/ProductDetail/Cree-Inc/XPEPHR-L1-0000-00801/?qs=3izLlwrMQ7lAtbsWL38zog%3D%3D) | | NIR | 730 nm | Cree, Inc. | XPEFAR-L1-0000-00601 | CREEXPE-FRD-3 | $12.00 | [LEDSupply](https://www.ledsupply.com/leds/cree-xlamp-xpe-high-power-led-star) | [DigiKey](https://www.digikey.com/en/products/detail/cree-inc/XPEFAR-L1-0000-00601/5303643) [Mouser](https://www.mouser.com/ProductDetail/Cree-Inc/XPEFAR-L1-0000-00601?qs=k72kBymvut%252B0JKg4b6%252BzNg%3D%3D) | -- cgit v1.2.3 From 0e2245384e9c27a96c7de428a07bf12f6ba1e66e Mon Sep 17 00:00:00 2001 From: plampkin <83132062+plampkin@users.noreply.github.com> Date: Tue, 18 May 2021 21:56:11 -0500 Subject: Update README.md --- photoreactor-base/README.md | 2 +- 1 file changed, 1 insertion(+), 1 deletion(-) diff --git a/photoreactor-base/README.md b/photoreactor-base/README.md index 60549ac..3417e62 100644 --- a/photoreactor-base/README.md +++ b/photoreactor-base/README.md @@ -14,7 +14,7 @@ Please see the fabrication and operation guide for LED star installation instruc | standoffs for PCB | RAF | 4505-440-AL | $1.00 | [DigiKey](https://www.digikey.com/en/products/detail/raf-electronic-hardware/4505-440-AL/7680509) [Newark](https://www.newark.com/raf-electronic-hardware/4505-440-al/no-plate-hex-male-female-standoffs/dp/95Y3120?st=4505-440-al) | | LED star heatsink | Ohmite | SV-LED-113E | $3.00 | [DigiKey](https://www.digikey.com/en/products/detail/ohmite/SV-LED-113E/2509399) | | LED star | Various (see `photon-source-leds` directory) | -| heat-set inserts | Virtjoule | | $0.00 | [Amazon](https://www.amazon.com/gp/product/B07BH5X252/ref=ppx_yo_dt_b_asin_title_o09_s00?ie=UTF8&psc=1) | +| heat-set inserts | Virtjoule | | $12.00 | [Amazon](https://www.amazon.com/gp/product/B07BH5X252/ref=ppx_yo_dt_b_asin_title_o09_s00?ie=UTF8&psc=1) | | fan | Noctua | NF-A12x15 PWM | $20.00 | [Amazon](https://www.amazon.com/Noctua-NF-A12x15-PWM-Premium-Quiet/dp/B071W6HJP6) | | 1/4" screws | Fastenal | 0146455 | | | 3/4" screws | Fastenal | 72490 | | -- cgit v1.2.3 From 841db2c36b6ef3d500f14674723ca7c85af5be22 Mon Sep 17 00:00:00 2001 From: Philip Lampkin Date: Wed, 19 May 2021 00:00:42 -0500 Subject: removed Logos 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b/fabrication-and-operation-instructions/tap-heatsink.jpg deleted file mode 100644 index 3d9ca04..0000000 Binary files a/fabrication-and-operation-instructions/tap-heatsink.jpg and /dev/null differ diff --git a/fabrication-and-operation-instructions/wpp-fabrication-operation.pdf b/fabrication-and-operation-instructions/wpp-fabrication-operation.pdf index 66abf3a..8e66b6d 100644 Binary files a/fabrication-and-operation-instructions/wpp-fabrication-operation.pdf and b/fabrication-and-operation-instructions/wpp-fabrication-operation.pdf differ diff --git a/fabrication-and-operation-instructions/wpp-fabrication-operation.tex b/fabrication-and-operation-instructions/wpp-fabrication-operation.tex index 0ceeb4e..492c57d 100644 --- a/fabrication-and-operation-instructions/wpp-fabrication-operation.tex +++ b/fabrication-and-operation-instructions/wpp-fabrication-operation.tex @@ -54,7 +54,7 @@ % title \title{Wisconsin Photoreactor Platform\\Fabrication and Operation Guide} -\author{Philip P. Lampkin, Blaise J. Thompson, Samuel H. Gellman*} +\author{Philip P. Lampkin, Blaise J. Thompson and Samuel H. Gellman*} \date{\today} @@ -594,6 +594,6 @@ Care must be taken to use safety glasses protective against the specific emissio \section{Acknowledgments} -We thank Dr. Ilia Guzei for photography. We are grateful to Sebastian Thompson for help in production of custom LED stars. +We thank Dr. Ilia A. Guzei for photography. We are grateful to Sebastian Thompson for help in production of custom LED stars. \end{document} -- cgit v1.2.3 From e586f494b9f187485a54718279c9040abf173ce9 Mon Sep 17 00:00:00 2001 From: Philip Lampkin Date: Wed, 19 May 2021 17:28:38 -0500 Subject: updated base graphic --- photoreactor-base/base.jpeg | Bin 0 -> 3669264 bytes photoreactor-base/base.jpg | Bin 3669264 -> 0 bytes 2 files changed, 0 insertions(+), 0 deletions(-) create mode 100644 photoreactor-base/base.jpeg delete mode 100755 photoreactor-base/base.jpg diff --git a/photoreactor-base/base.jpeg b/photoreactor-base/base.jpeg new file mode 100644 index 0000000..6e87c43 Binary files /dev/null and b/photoreactor-base/base.jpeg differ diff --git a/photoreactor-base/base.jpg b/photoreactor-base/base.jpg deleted file mode 100755 index 6e87c43..0000000 Binary files a/photoreactor-base/base.jpg and /dev/null differ -- cgit v1.2.3 From 26b07a0627b170d5a16b0aa70c4c1a7a5479ebdd Mon Sep 17 00:00:00 2001 From: plampkin <83132062+plampkin@users.noreply.github.com> Date: Wed, 19 May 2021 17:29:55 -0500 Subject: Update README.md --- photoreactor-base/README.md | 2 +- 1 file changed, 1 insertion(+), 1 deletion(-) diff --git a/photoreactor-base/README.md b/photoreactor-base/README.md index 3417e62..dac20d4 100644 --- a/photoreactor-base/README.md +++ b/photoreactor-base/README.md @@ -1,6 +1,6 @@ # WPP Standardized Base -![WPP base](./base.jpg) +![WPP base](./base.jpeg) The core structure of the Wisconsin Photoreactor Platform. Each reactor shares this component. It has a 130 mm by 130 mm footprint and is compatible with typical laboratory stir plates. -- cgit v1.2.3 From 1b9bbf10931ae958419241cf26a974f59eb9ee6e Mon Sep 17 00:00:00 2001 From: Philip Lampkin Date: Wed, 19 May 2021 18:14:09 -0500 Subject: updated fab/op guide title page --- .../wpp-fabrication-operation.pdf | Bin 46759065 -> 46758479 bytes .../wpp-fabrication-operation.tex | 21 ++++++++++++--------- 2 files changed, 12 insertions(+), 9 deletions(-) diff --git a/fabrication-and-operation-instructions/wpp-fabrication-operation.pdf b/fabrication-and-operation-instructions/wpp-fabrication-operation.pdf index 8e66b6d..7605705 100644 Binary files a/fabrication-and-operation-instructions/wpp-fabrication-operation.pdf and b/fabrication-and-operation-instructions/wpp-fabrication-operation.pdf differ diff --git a/fabrication-and-operation-instructions/wpp-fabrication-operation.tex b/fabrication-and-operation-instructions/wpp-fabrication-operation.tex index 492c57d..bad26f7 100644 --- a/fabrication-and-operation-instructions/wpp-fabrication-operation.tex +++ b/fabrication-and-operation-instructions/wpp-fabrication-operation.tex @@ -52,9 +52,10 @@ \usepackage[numbers]{natbib} % title -\title{Wisconsin Photoreactor Platform\\Fabrication and Operation Guide} +\title{% + \textbf{A Versatile Open-source Photoreactor Architecture\\ for Photocatalysis Across the Visible Spectrum}} -\author{Philip P. Lampkin, Blaise J. Thompson and Samuel H. Gellman*} +\author{\textbf{Philip P. Lampkin, Blaise J. Thompson and Samuel H. Gellman*} \\ \textit{University of Wisconsin-Madison, Madison, Wisconsin, 53706} \\ \\ \textit{Email: \href{mailto:gellman@chem.wisc.edu}{gellman@chem.wisc.edu}}} \date{\today} @@ -62,6 +63,8 @@ \maketitle +\centering{\textbf{\LARGE Wisconsin Photoreactor Platform\\Fabrication and Operation Guide}}} + \includegraphics[width=\textwidth]{"../coverart.png"} \tableofcontents @@ -85,7 +88,7 @@ Each component is highly versatile, and apparatus assembly is fully modular (Fig Through variation of each component, one can quickly produce bespoke WPP devices to meet specific research needs. The WPP is a living project. -We encourage duplication and modification of our designs. +We encourage duplication, modification and expansion of our designs. If you would like to contribute to the WPP project or notice a problem, please consider opening a pull request or issue on GitHub. \section{Fabrication} @@ -121,7 +124,7 @@ A list of LED stars tested with the WPP platform is available in the 'photon-sou It is easiest to use LED stars with pre-mounted LEDs. Otherwise, you can fabricate custom LED stars with discrete LEDs and bare LED star circuit boards. Custom LED star production requires a reflow oven. -All LED stars must be mounted that have LEDs with a maximum drive current of 1000 mA. +All LEDs must have a maximum drive current of 1000 mA or higher. \begin{figure}[H] \includegraphics[width=\textwidth]{"./fig3.png"} @@ -150,7 +153,7 @@ The same base is shared by all WPP devices. When interacting with the design files in our repository you will see several filetypes. We have designed the WPP enclosure using Autodesk's Fusion 360 and included f3d design files for those who wish to extend or modify our designs. -Interacting with f3d files requires a Fusion 360 license, which is free to students and educators. +Interacting with f3d files requires a Fusion 360 license, which is free for students and educators. You will also find stl files in the repository. These are common 3D-model exchange files that can be viewed with 3D modeling programs or printed with 3D-printers. @@ -258,12 +261,12 @@ Your reaction module is now ready for use. \end{figure} A WPP device can be driven using an analog driver circuit board, a digital driver circuit board or a simple electronic circuit with a commercial LED driver (Figure 10). -All provide power to the cooling fan and constant current to the LEDs. +All provide power to the cooling fan and current to the LEDs. All utilize 1000 mA LED drivers. \textbf{\textit{Each provides different configurational capabilities.}} Both driver boards are built around Mean Well's LDD-1000L LED driver module. -This module delivers constant current up to one amp. +This module delivers current up to one amp. The current delivered can be controlled electronically in several different ways. Users wishing to understand this design should refer to Mean Well's datasheet. Refer to the "analog-driver-board" and "digital-driver-board" directories in the online repository for design files for each board. @@ -302,7 +305,7 @@ You may upload these zip files to PCB manufacturers when ordering copies of our \caption{(A) WPP devices fitted with analog driver boards connected in series. (B) Multimeter and WPP apparatus fitted with analog driver board. (C) Connection of multimeter to test points. (D) WPP apparatus at ~60 percent light intensity (1.5 V test point voltage)} \end{figure} -\textbf{\textit{Through use of the analog driver board, one can reproducibly control WPP device light intensity.}} +\textbf{\textit{Through use of the analog driver board, one can reproducibly control WPP device light intensity via modulation of drive current.}} This control is achieved through adjustment of the board-mounted potentiometer. No firmware is required, and multiple WPP reactors can be connected in series to a single power source (Figure 11A). However, fan speed isn’t adjustable and is maintained at maximum. @@ -382,7 +385,7 @@ The analog driver board is now ready for use. \label{FIG:digital-driver-network} \end{figure} -\textbf{\textit{Through use of the digital driver board, one can control WPP device light intensity and fan speed.}} This control is achieved by interfacing a control unit, like an Arduino Uno, to the digital driver board using custom software. Multiple WPP devices with digital driver boards can be connected to a single control unit and power supply (Figure 15). Open-source firmware for interfacing digital driver boards with an Arduino Uno control unit is provided in the project repository. Other peripherals can be connected to digital driver boards to expand functionality, but firmware must be produced to interface with them. +\textbf{\textit{Through use of the digital driver board, one can control WPP device light intensity and fan speed using pulse width modulation.}} This control is achieved by interfacing a control unit, like an Arduino Uno, to the digital driver board using custom firmware. Multiple WPP devices with digital driver boards can be connected to a single control unit and power supply (Figure 15). Open-source firmware for interfacing digital driver boards with an Arduino Uno control unit is provided in the project repository. Other peripherals can be connected to digital driver boards to expand functionality, but firmware must be produced to interface with them. To fabricate a digital driver board, first order digital driver PCBs from a PCB manufacturer. You will be sent bare boards of the type seen in Figure 16A. -- cgit v1.2.3 From cfcd9ac0d312c67b11f9bb35693fb4da366f338d Mon Sep 17 00:00:00 2001 From: Philip Lampkin Date: Mon, 24 May 2021 10:48:20 -0500 Subject: added light shield --- photoreactor-light-shield/light_shield.f3d | Bin 0 -> 2058747 bytes photoreactor-light-shield/light_shield.stl | Bin 0 -> 122284 bytes 2 files changed, 0 insertions(+), 0 deletions(-) create mode 100644 photoreactor-light-shield/light_shield.f3d create mode 100644 photoreactor-light-shield/light_shield.stl diff --git a/photoreactor-light-shield/light_shield.f3d b/photoreactor-light-shield/light_shield.f3d new file mode 100644 index 0000000..7572bb0 Binary files /dev/null and b/photoreactor-light-shield/light_shield.f3d differ diff --git a/photoreactor-light-shield/light_shield.stl b/photoreactor-light-shield/light_shield.stl new file mode 100644 index 0000000..aa06818 Binary files /dev/null and b/photoreactor-light-shield/light_shield.stl differ -- cgit v1.2.3 From 8945a9d808ef2d4797342777864425d4bc76d828 Mon Sep 17 00:00:00 2001 From: plampkin <83132062+plampkin@users.noreply.github.com> Date: Mon, 24 May 2021 11:34:17 -0500 Subject: Update README.md --- README.md | 9 ++++++--- 1 file changed, 6 insertions(+), 3 deletions(-) diff --git a/README.md b/README.md index ce79834..f3acb07 100644 --- a/README.md +++ b/README.md @@ -22,8 +22,9 @@ This repository is being mirrored to several version control systems in an attem The Wisconsin Photoreactor Platform is for use by trained chemists. WPP apparatuses utilize high-intensity light emitting diodes (LED) that can cause eye damage if proper safety precautions are not observed. -Light-filtering safety glasses should be worn whenever a WPP apparatus photon source is powered. -Care must be taken to use safety glasses protective against the specific emission wavelengths of a photon source. +A Light-blocking shield should be utilized whenever operating a WPP apparatus. +Care must be taken to ensure the light-blocking shield employed adequately blocks light emitted by a WPP photon source from directly reaching a user. +Use of light-filtering safety glasses alongside a light-blocking shield can provide additional protection. ## Fabrication and Operation Instructions @@ -32,10 +33,12 @@ Please see [wpp-fabrication-operation.pdf](./fabrication-and-operation-instructi ## Enclosure -The WPP is designed around a mechanically robust 3D printed enclosure. +The WPP is designed around a mechanically robust and simple 3D printed enclosure. Every WPP device has the same base, see directory `photoreactor-base`. WPP reaction modules are meant to be switched based on the reaction vessel used. See directory `photoreactor-reaction-modules` for our growing collection of reaction modules for common vessel types. +For safe WPP device operation, a light blocking shield is recommended. +See directory `photoreactor-light-shield`, for a 3D-printable light-blocking cover for WPP devices. ## Electronics -- cgit v1.2.3 From 51a09055210aac1052da104f9b9ba5dfccadf438 Mon Sep 17 00:00:00 2001 From: plampkin <83132062+plampkin@users.noreply.github.com> Date: Mon, 24 May 2021 11:36:34 -0500 Subject: Update README.md --- README.md | 1 + 1 file changed, 1 insertion(+) diff --git a/README.md b/README.md index f3acb07..3b69949 100644 --- a/README.md +++ b/README.md @@ -34,6 +34,7 @@ Please see [wpp-fabrication-operation.pdf](./fabrication-and-operation-instructi ## Enclosure The WPP is designed around a mechanically robust and simple 3D printed enclosure. + Every WPP device has the same base, see directory `photoreactor-base`. WPP reaction modules are meant to be switched based on the reaction vessel used. See directory `photoreactor-reaction-modules` for our growing collection of reaction modules for common vessel types. -- cgit v1.2.3 From 06ee1a51239553b42a32317ba6d4fb0e725a52f8 Mon Sep 17 00:00:00 2001 From: plampkin <83132062+plampkin@users.noreply.github.com> Date: Mon, 24 May 2021 12:22:23 -0500 Subject: Create README.md --- photoreactor-light-shield/README.md | 11 +++++++++++ 1 file changed, 11 insertions(+) create mode 100644 photoreactor-light-shield/README.md diff --git a/photoreactor-light-shield/README.md b/photoreactor-light-shield/README.md new file mode 100644 index 0000000..8386569 --- /dev/null +++ b/photoreactor-light-shield/README.md @@ -0,0 +1,11 @@ +# WPP light shield + +![WPP cover](./cover.png) + +A 3D-printable, light-blocking cover for Wisconsin Photoreactor Platform devices. +This generic cover module fits all WPP reaction modules. +No customization of cover geometry is required. + +The WPP light shield provides protection from direct exposure to light from WPP photon sources. +Printing the WPP light shield using black filament is recommended to reduce light bounce. +Use of light-filtering safety glasses or additional light-blocking shields alongside the WPP light shield module is recommended for additional protection. -- cgit v1.2.3 From d0956dbf2323d46c2d91c9bd78b97747356fb9c5 Mon Sep 17 00:00:00 2001 From: plampkin <83132062+plampkin@users.noreply.github.com> Date: Mon, 24 May 2021 12:38:25 -0500 Subject: Update README.md --- photon-source-leds/README.md | 22 +++++++++++----------- 1 file changed, 11 insertions(+), 11 deletions(-) diff --git a/photon-source-leds/README.md b/photon-source-leds/README.md index 22386fd..89dfd30 100644 --- a/photon-source-leds/README.md +++ b/photon-source-leds/README.md @@ -8,17 +8,17 @@ WPP-compatible custom LED stars mounted with 3.5 mm surface mount LEDs of any wa ## List of compatible commercial LED stars -| color | max emission | manufacturer | manufacturer part number | LEDsupply LED star part number | LEDsupply price | LED Star vendors | LED vendors | -| :------------- | :----------- | :----------- | :----------------------- | :----------------------------- | :-------------- | :--------------- | :------------ | -| UVA | 365 nm | Inolux | IN-C39CTOU2 | N/A (mounted by user) | N/A | N/A | [DigiKey](https://www.digikey.com/en/products/detail/inolux/IN-C39CTOU2/9681227) [Mouser](https://www.mouser.com/ProductDetail/Inolux/IN-C39CTOU2/?qs=qSfuJ%252Bfl%2Fd4759YPTEyoag%3D%3D) | -| Violet | 395 nm | Inolux | IN-C39CTOU5 | N/A (mounted by user) | N/A | N/A | [DigiKey](https://www.digikey.com/en/products/detail/inolux/IN-C39CTOU5/9681233) [Mouser](https://www.mouser.com/ProductDetail/Inolux/IN-C39CTOU5/?qs=qSfuJ%252Bfl%2Fd6BLbca08ZG2g%3D%3D) | -| Blue | 450 nm | Cree, Inc. | XTEARY-00-0000-000000N09 | CREEXTE-ROY-3 | $10.10 | [LEDSupply](https://www.ledsupply.com/leds/cree-xlamp-xt-e-royal-blue-leds) | [DigiKey](https://www.digikey.com/en/products/detail/cree-inc/XTEARY-00-0000-000000N09/3744336) [Mouser](https://www.mouser.com/ProductDetail/Cree-Inc/XTEARY-00-0000-000000N09?qs=ygRr%2Ftkhtevu4HqMzfGc3w%3D%3D) | -| Cyan | 495 nm | Luxeon | LXML-PE01-0080 | 07007-PE000-K | $12.60 | [LEDSupply](https://www.ledsupply.com/leds/luxeon-rebel-color-leds) | [DigiKey](https://www.digikey.com/en/products/detail/lumileds/LXML-PE01-0080/3961255) [Mouser](https://www.mouser.com/ProductDetail/Lumileds/LXML-PE01-0080/?qs=7Vwje68bFtO%2F0g2M%252BAMdYQ%3D%3D) | -| Green | 530 nm | Cree, Inc. | XPEBGR-L1-0000-00D01 | CREEXPE2-GRN-3 | $10.50 | [LEDSupply](https://www.ledsupply.com/leds/cree-xlamp-xp-e2-color-high-power-led-star) | [DigiKey](https://www.digikey.com/en/products/detail/cree-inc/XPEBGR-L1-0000-00D01/4177200) [Mouser](https://www.mouser.com/ProductDetail/Cree-Inc/XPEBGR-L1-0000-00D01/?qs=rHlcMk0NooK%2FtCgm9PQ0pQ%3D%3D) | -| Amber | 595 nm | Luxeon | LXML-PL01-0060 | 07007-PL000-F | $12.60 | [LEDSupply](https://www.ledsupply.com/leds/luxeon-rebel-color-leds) | [DigiKey](https://www.digikey.com/en/products/detail/lumileds/LXML-PL01-0050/3961256) [Mouser](https://www.mouser.com/ProductDetail/Lumileds/LXML-PL01-0060?qs=7Vwje68bFtP0H6dN9OA%2FuA%3D%3D) | -| Orange | 620 nm | Cree, Inc. | XPEBRO-L1-0000-00901 | CREEXPE2-RDO-3 | $10.50 | [LEDSupply](https://www.ledsupply.com/leds/cree-xlamp-xp-e2-color-high-power-led-star) | [DigiKey](https://www.digikey.com/en/products/detail/cree-inc/XPEBRO-L1-0000-00901/4177164) [Mouser](https://www.mouser.com/ProductDetail/Cree-Inc/XPEBRO-L1-0000-00901?qs=rHlcMk0NooLQklUEc3IqMg%3D%3D) | -| Red | 660 nm | Cree, Inc. | XPEPHR-L1-0000-00801 | CREEXPE-DRD-3 | $10.50 | [LEDSupply](https://www.ledsupply.com/leds/cree-xlamp-xpe-high-power-led-star) | [DigiKey](https://www.digikey.com/en/products/detail/cree-inc/XPEPHR-L1-0000-00801/4895013) [Mouser](https://www.mouser.com/ProductDetail/Cree-Inc/XPEPHR-L1-0000-00801/?qs=3izLlwrMQ7lAtbsWL38zog%3D%3D) | -| NIR | 730 nm | Cree, Inc. | XPEFAR-L1-0000-00601 | CREEXPE-FRD-3 | $12.00 | [LEDSupply](https://www.ledsupply.com/leds/cree-xlamp-xpe-high-power-led-star) | [DigiKey](https://www.digikey.com/en/products/detail/cree-inc/XPEFAR-L1-0000-00601/5303643) [Mouser](https://www.mouser.com/ProductDetail/Cree-Inc/XPEFAR-L1-0000-00601?qs=k72kBymvut%252B0JKg4b6%252BzNg%3D%3D) | +| color | max emission (nm) | max current (mA) | manufacturer | manufacturer part number | LEDsupply LED star part number | LEDsupply price | LED Star vendors | LED vendors | +| :------------- | :----------- | :----------- | :----------- | :----------------------- | :----------------------------- | :-------------- | :--------------- | :------------ | +| UVA | 365 | 1200 | Inolux | IN-C39CTOU2 | N/A (mounted by user) | N/A | N/A | [DigiKey](https://www.digikey.com/en/products/detail/inolux/IN-C39CTOU2/9681227) [Mouser](https://www.mouser.com/ProductDetail/Inolux/IN-C39CTOU2/?qs=qSfuJ%252Bfl%2Fd4759YPTEyoag%3D%3D) | +| Violet | 395 | 1200 | Inolux | IN-C39CTOU5 | N/A (mounted by user) | N/A | N/A | [DigiKey](https://www.digikey.com/en/products/detail/inolux/IN-C39CTOU5/9681233) [Mouser](https://www.mouser.com/ProductDetail/Inolux/IN-C39CTOU5/?qs=qSfuJ%252Bfl%2Fd6BLbca08ZG2g%3D%3D) | +| Blue | 450 | 1500 | Cree, Inc. | XTEARY-00-0000-000000N09 | CREEXTE-ROY-3 | $10.10 | [LEDSupply](https://www.ledsupply.com/leds/cree-xlamp-xt-e-royal-blue-leds) | [DigiKey](https://www.digikey.com/en/products/detail/cree-inc/XTEARY-00-0000-000000N09/3744336) [Mouser](https://www.mouser.com/ProductDetail/Cree-Inc/XTEARY-00-0000-000000N09?qs=ygRr%2Ftkhtevu4HqMzfGc3w%3D%3D) | +| Cyan | 495 | 1000 | Luxeon | LXML-PE01-0080 | 07007-PE000-K | $12.60 | [LEDSupply](https://www.ledsupply.com/leds/luxeon-rebel-color-leds) | [DigiKey](https://www.digikey.com/en/products/detail/lumileds/LXML-PE01-0080/3961255) [Mouser](https://www.mouser.com/ProductDetail/Lumileds/LXML-PE01-0080/?qs=7Vwje68bFtO%2F0g2M%252BAMdYQ%3D%3D) | +| Green | 530 | 1000 | Cree, Inc. | XPEBGR-L1-0000-00D01 | CREEXPE2-GRN-3 | $10.50 | [LEDSupply](https://www.ledsupply.com/leds/cree-xlamp-xp-e2-color-high-power-led-star) | [DigiKey](https://www.digikey.com/en/products/detail/cree-inc/XPEBGR-L1-0000-00D01/4177200) [Mouser](https://www.mouser.com/ProductDetail/Cree-Inc/XPEBGR-L1-0000-00D01/?qs=rHlcMk0NooK%2FtCgm9PQ0pQ%3D%3D) | +| Amber | 595 | 1000 | Luxeon | LXML-PL01-0060 | 07007-PL000-F | $12.60 | [LEDSupply](https://www.ledsupply.com/leds/luxeon-rebel-color-leds) | [DigiKey](https://www.digikey.com/en/products/detail/lumileds/LXML-PL01-0050/3961256) [Mouser](https://www.mouser.com/ProductDetail/Lumileds/LXML-PL01-0060?qs=7Vwje68bFtP0H6dN9OA%2FuA%3D%3D) | +| Orange | 620 | 1000 | Cree, Inc. | XPEBRO-L1-0000-00901 | CREEXPE2-RDO-3 | $10.50 | [LEDSupply](https://www.ledsupply.com/leds/cree-xlamp-xp-e2-color-high-power-led-star) | [DigiKey](https://www.digikey.com/en/products/detail/cree-inc/XPEBRO-L1-0000-00901/4177164) [Mouser](https://www.mouser.com/ProductDetail/Cree-Inc/XPEBRO-L1-0000-00901?qs=rHlcMk0NooLQklUEc3IqMg%3D%3D) | +| Red | 660 | 1000 | Cree, Inc. | XPEPHR-L1-0000-00801 | CREEXPE-DRD-3 | $10.50 | [LEDSupply](https://www.ledsupply.com/leds/cree-xlamp-xpe-high-power-led-star) | [DigiKey](https://www.digikey.com/en/products/detail/cree-inc/XPEPHR-L1-0000-00801/4895013) [Mouser](https://www.mouser.com/ProductDetail/Cree-Inc/XPEPHR-L1-0000-00801/?qs=3izLlwrMQ7lAtbsWL38zog%3D%3D) | +| NIR | 730 | 1000 | Cree, Inc. | XPEFAR-L1-0000-00601 | CREEXPE-FRD-3 | $12.00 | [LEDSupply](https://www.ledsupply.com/leds/cree-xlamp-xpe-high-power-led-star) | [DigiKey](https://www.digikey.com/en/products/detail/cree-inc/XPEFAR-L1-0000-00601/5303643) [Mouser](https://www.mouser.com/ProductDetail/Cree-Inc/XPEFAR-L1-0000-00601?qs=k72kBymvut%252B0JKg4b6%252BzNg%3D%3D) | All prices are in USD. In general, prices are overestimates, thereby providing an upper estimate on cost. -- cgit v1.2.3 From 17e0c34300d2197074850d6d6a2e3abf75652cad Mon Sep 17 00:00:00 2001 From: plampkin <83132062+plampkin@users.noreply.github.com> Date: Mon, 24 May 2021 13:09:33 -0500 Subject: Update README.md --- README.md | 2 +- 1 file changed, 1 insertion(+), 1 deletion(-) diff --git a/README.md b/README.md index 3b69949..5bb0405 100644 --- a/README.md +++ b/README.md @@ -22,7 +22,7 @@ This repository is being mirrored to several version control systems in an attem The Wisconsin Photoreactor Platform is for use by trained chemists. WPP apparatuses utilize high-intensity light emitting diodes (LED) that can cause eye damage if proper safety precautions are not observed. -A Light-blocking shield should be utilized whenever operating a WPP apparatus. +A light-blocking shield should be utilized whenever operating a WPP apparatus. Care must be taken to ensure the light-blocking shield employed adequately blocks light emitted by a WPP photon source from directly reaching a user. Use of light-filtering safety glasses alongside a light-blocking shield can provide additional protection. -- cgit v1.2.3 From ef2a1f94cfe58be8bfa42e51b94c33f18f999289 Mon Sep 17 00:00:00 2001 From: plampkin <83132062+plampkin@users.noreply.github.com> Date: Mon, 24 May 2021 17:45:17 -0500 Subject: Update README.md --- photoreactor-light-shield/README.md | 2 +- 1 file changed, 1 insertion(+), 1 deletion(-) diff --git a/photoreactor-light-shield/README.md b/photoreactor-light-shield/README.md index 8386569..17e00b5 100644 --- a/photoreactor-light-shield/README.md +++ b/photoreactor-light-shield/README.md @@ -7,5 +7,5 @@ This generic cover module fits all WPP reaction modules. No customization of cover geometry is required. The WPP light shield provides protection from direct exposure to light from WPP photon sources. -Printing the WPP light shield using black filament is recommended to reduce light bounce. +Printing the WPP light shield cover module using black filament is recommended to reduce light bounce. Use of light-filtering safety glasses or additional light-blocking shields alongside the WPP light shield module is recommended for additional protection. -- cgit v1.2.3 From b3819531b085beb4eb1248c676f0e174d26c1e5b Mon Sep 17 00:00:00 2001 From: Philip Lampkin Date: Wed, 26 May 2021 01:21:36 -0500 Subject: updated safety guide with light shield information --- fabrication-and-operation-instructions/fig24.png | Bin 0 -> 9218562 bytes .../wpp-fabrication-operation.pdf | Bin 46758479 -> 60576571 bytes .../wpp-fabrication-operation.tex | 25 +++++++++++++++------ 3 files changed, 18 insertions(+), 7 deletions(-) create mode 100644 fabrication-and-operation-instructions/fig24.png diff --git a/fabrication-and-operation-instructions/fig24.png b/fabrication-and-operation-instructions/fig24.png new file mode 100644 index 0000000..498647c Binary files /dev/null and b/fabrication-and-operation-instructions/fig24.png differ diff --git a/fabrication-and-operation-instructions/wpp-fabrication-operation.pdf b/fabrication-and-operation-instructions/wpp-fabrication-operation.pdf index 7605705..0ccf6fe 100644 Binary files a/fabrication-and-operation-instructions/wpp-fabrication-operation.pdf and b/fabrication-and-operation-instructions/wpp-fabrication-operation.pdf differ diff --git a/fabrication-and-operation-instructions/wpp-fabrication-operation.tex b/fabrication-and-operation-instructions/wpp-fabrication-operation.tex index bad26f7..4f0b32d 100644 --- a/fabrication-and-operation-instructions/wpp-fabrication-operation.tex +++ b/fabrication-and-operation-instructions/wpp-fabrication-operation.tex @@ -63,8 +63,6 @@ \maketitle -\centering{\textbf{\LARGE Wisconsin Photoreactor Platform\\Fabrication and Operation Guide}}} - \includegraphics[width=\textwidth]{"../coverart.png"} \tableofcontents @@ -222,7 +220,7 @@ Remember to use proper eye protection. A WPP reaction module consists of a reaction chamber and vessel holder. By modifying chamber height and adjusting holder geometry, one can produce modules compatible with reaction vessels of various types and sizes. -Fusion360 designs and stl models for modules compatible with 2-, 4-, 8- and 24-mL vials are provided in the 'photoreaction-modules' subdirectory of the project repository (Figure 8A—B). +Fusion360 designs and stl models for modules compatible with 2-, 4-, 8- and 24-mL vials are provided in the 'photoreactor-reaction-modules' subdirectory of the project repository (Figure 8A—B). Template reaction chamber and vessel holder Fusion360 designs are provided in the same directory. We encourage you to design your own reaction modules if those provided in the project repository do not meet your needs. @@ -510,7 +508,7 @@ Once a WPP apparatus is configured with the desired photon source, reaction modu \caption{A WPP apparatus with a 450 nm photon source, 4 mL reactor module and digital driver board on a standard laboratory stir plate conducting 6 simultaneous photoreactions in the multiple reaction configuration.} \end{figure} -To conduct a photoreaction using a WPP device, an assembled apparatus should be placed on a lab stir plate, to provide reaction mixture stirring, and reaction vessels should be inserted into the apparatus in the desired layout (Figure 8). +To conduct a photoreaction using a WPP device, an assembled apparatus should be placed on a lab stir plate, to provide reaction mixture stirring, and reaction vessels should be inserted into the apparatus in the desired layout (Figure 23). The 130 by 130 mm footprint of the WPP architecture is compatible with typical stir plates. A standard 12 V power supply can then be plugged into the reactor driver to turn on the device and start irradiation. A single 12V 2 A power supply is sufficient to drive 2 WPP devices simultaneously. @@ -592,11 +590,24 @@ This information enables reproduction WPP devices fitted with the simple LED dri \section{Safety} WPP reactors utilize high-intensity light emitting diodes (LED) that can cause eye damage if proper safety precautions are not observed. -Light-filtering safety glasses should be worn whenever a WPP apparatus photon source is powered. -Care must be taken to use safety glasses protective against the specific emission wavelengths of the photon source. + +A light-blocking shield should be utilized whenever operating a WPP apparatus. +Care must be taken to ensure the light-blocking shield employed adequately blocks light emitted by a WPP photon source from directly reaching a user. + +\begin{figure}[H] + \centering + \includegraphics[width=\textwidth/2]{"./fig24.png"} + \caption{WPP device fitted the provided light shield cover module printed in black PLA.} +\end{figure} + +A 3D printable light-blocking cover module for WPP devices is provided in the 'photoreactor-light-shield' subdirectory of the project repository. +The WPP light shield prevents direct exposure of users to light emitted by WPP photon sources. +We recommend printing the WPP light shield using black filament is recommended to reduce light bounce (Figure 24). + +Use of light-filtering safety glasses alongside a light-blocking shield can provide additional protection from high-intensity light. \section{Acknowledgments} -We thank Dr. Ilia A. Guzei for photography. We are grateful to Sebastian Thompson for help in production of custom LED stars. +We thank Dr. Ilia A. Guzei and Sebastian Thompson of UW-Madison for photography and help fabricating custom LED stars, respectively. \end{document} -- cgit v1.2.3 From b614982b0ee2ce70876a6a81de9051f1e9e874a9 Mon Sep 17 00:00:00 2001 From: Philip Lampkin Date: Wed, 26 May 2021 01:23:20 -0500 Subject: added light shield photo to subdirectory --- photoreactor-light-shield/cover.png | Bin 0 -> 9218562 bytes 1 file changed, 0 insertions(+), 0 deletions(-) create mode 100644 photoreactor-light-shield/cover.png diff --git a/photoreactor-light-shield/cover.png b/photoreactor-light-shield/cover.png new file mode 100644 index 0000000..498647c Binary files /dev/null and b/photoreactor-light-shield/cover.png differ -- cgit v1.2.3 From 0eee28f19478005a46154c7e17adb52230f29790 Mon Sep 17 00:00:00 2001 From: Philip Lampkin Date: Wed, 26 May 2021 01:53:09 -0500 Subject: updated operations guide title page --- .../wpp-fabrication-operation.pdf | Bin 60576571 -> 60575926 bytes .../wpp-fabrication-operation.tex | 6 ++++-- 2 files changed, 4 insertions(+), 2 deletions(-) diff --git a/fabrication-and-operation-instructions/wpp-fabrication-operation.pdf b/fabrication-and-operation-instructions/wpp-fabrication-operation.pdf index 0ccf6fe..5629032 100644 Binary files a/fabrication-and-operation-instructions/wpp-fabrication-operation.pdf and b/fabrication-and-operation-instructions/wpp-fabrication-operation.pdf differ diff --git a/fabrication-and-operation-instructions/wpp-fabrication-operation.tex b/fabrication-and-operation-instructions/wpp-fabrication-operation.tex index 4f0b32d..c56ffa0 100644 --- a/fabrication-and-operation-instructions/wpp-fabrication-operation.tex +++ b/fabrication-and-operation-instructions/wpp-fabrication-operation.tex @@ -56,13 +56,15 @@ \textbf{A Versatile Open-source Photoreactor Architecture\\ for Photocatalysis Across the Visible Spectrum}} \author{\textbf{Philip P. Lampkin, Blaise J. Thompson and Samuel H. Gellman*} \\ \textit{University of Wisconsin-Madison, Madison, Wisconsin, 53706} \\ \\ \textit{Email: \href{mailto:gellman@chem.wisc.edu}{gellman@chem.wisc.edu}}} - \date{\today} \begin{document} \maketitle - +\centering{\textbf{{\Large Wisconsin Photoreactor Platform\\ Fabrication and Operation Guide}}} + +\vspace{10mm} %5mm vertical space + \includegraphics[width=\textwidth]{"../coverart.png"} \tableofcontents -- cgit v1.2.3